Chapter 5 GLC-美国食品药品管理局标准-FDA

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1、PesticideAnalyticalManualVol.ISECTION500Chapter1RegulatoryOperationsChapter2GeneralAnalyticalOperationsandInformationChapter3Chapter4MulticlassSelectiveMRMsMRMsChapter5GLCChapter6HPLCTableofContentspagedate501:GeneralInformation501A:Principles501-11/94501B:EquipmentforGLC501

2、-11/94GasChromatographicComponents501-11/94OtherApparatus501-21/94ReagentsandGases501-31/94501C:ResidueMethodologyforGLCDetermination501-31/94Cleanup501-41/94ReagentBlanks501-51/94ChoiceofSolvent501-61/94501D:InjectionTechniques501-61/94ManualInjection501-61/94Autoinjectors5

3、01-71/94501E:ReferenceStandards501-81/94References501-81/94TransmittalNo.96-E1(9/96)FormFDA2905a(6/92)500–1SECTION500PesticideAnalyticalManualVol.Ipagedate502:Columns502A:Introduction502-11/94ColumnSpecifications502-11/94ColumnParameters502-21/94502B:PackedColumns502-61/94Co

4、mponentsofPackedColumns502-61/94PreparationofPackedColumns502-81/94InstallationofPackedColumns502-91/94ConditioningofPackedColumns502-101/94RejuvenationofPackedColumns502-101/94CriteriaforAcceptablePackedColumns502-111/94RecommendedOperatingProcedures502-121/94forPackedColum

5、ns502C:OpenTubularCapillaryColumns502-131/94ColumnDescription502-141/94InjectionontoCapillaryColumns502-161/94CapillaryColumnSystems502-161/94InstallationandConditioningof502-201/94CapillaryColumnsRejuvenationofCapillaryColumns502-211/94RecommendedOperatingProcedurefor502-22

6、1/94WideBoreColumns(Isothermal)ApparatusandReagents502-221/94SystemStartupandInspection502-251/94References502-251/94503:Detectors503A:Introduction503-11/94DefinitionsofDetectorCharacteristics503-11/94503B:ElectronCaptureDetector503-21/94Principles503-31/94Design503-31/94App

7、aratusandReagents503-31/94DetectorCharacteristics503-41/94OtherInfluencesonDetectorPerformance503-71/94RecommendedOperatingProcedures503-81/94503C:FlamePhotometricDetector503-91/94Principles503-91/94Design503-91/94ApparatusandReagents503-101/94DetectorCharacteristics503-101/

8、94OtherInfluencesonDetectorPerformance503-111/94RecommendedOperatingProcedu