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ID:32008806
大小:7.59 MB
页数:63页
时间:2019-01-30
《天然硅酸盐纳米管复合催化剂的制备与其热催化性能-研究》由会员上传分享,免费在线阅读,更多相关内容在教育资源-天天文库。
1、郑州大学硕士学位论文ABSTRACTNanomaterialswiththedistinct.ProPertyhavebeenaPPliedgraduallyindiversedomain.WhilethesynthesizednanomaterialshavesomedefeetssuehaslowoutPut,higheost.Whatmore,thesematerialsPollutetheenvironmentseverely.Allthedefectsrestrietthedevelo
2、PmentandaPPlieationofsynthesizednanomaterials.ThenaturalnanometermineraleanbecomerarenanomaterialswithexeellentnaturesafterbeendealedwithProPeriy.Thenaturalnanometermineral15suPeriortothesynthesizednanomaterialsinoutPutandcost.InthisPaPer,thenatUrals
3、ilieatenanometermineral(HN劝wasselectedandeharaeterizedbymeansofScanningelectronmicroseoPe(SEM),TransmissionelectronmicroscoPe(TEM),EnergydisPersivesPeetroscoPy(EDS),X一raydi价action(XRD),InftaredSPectroseoPy(IR),Brunauer-Emmer-Teller(BET),DifferentialS
4、canningCalorimetry(DSC)andThermogravimetrie(TG).ItwasalsostudiedascatalysissuPPortsandusedto,analysisPreParecomP0undeatalyst.MicrostructureofHNTsuchascrystallograPhiestructure,grainsize,Particlemorphology,elementanalysisandthermalstabilizationwerecha
5、racterized.TheresultsindicatedthatHNTwashighqualitymineral.IthadashorteylindriealshaPeandatubularmorphology,highsPecifiesurfacearea,aswellasstrengthandexcellentthermalstability,whichmakesitusedascatalysissuPPorts.AceordingtotheresultsofDSC,wegottheea
6、talytiecharacteristicofHNTPowderonthehightemPeraturedecomPositionofammoniumPerehlorate(AP).ItcouldmakethetemPeratureofhightemPeratureexothermiePeakofApdeerease48oC.HNTINio,HNT/Mn02andHNT/ZnocomPositeParticleswerePreParedbythemethodsoffastPreciPitatio
7、n,redoxandstatieadsorptionresPeetively.ThecomPositePartielesobtainedhadbeencharacterizedbyXRD,TEMandHighResolutionTransmissionElectronMicroscoPe(HRTEM).Theresultsshowedthatthenano-P叭icleswerecoateduniformlyonthesuri妞ceofHNT.TOanalyzethecatalytieeffee
8、tofthecomPositeParticlesonthethermaldecomPositionofAP,thecomParisonsamPle大郑州大学硕士学位论文bysimPlymixingmetalormetaloxidePartielesandHNTwithAPresPeetively,hadbeenPrePared.DSCwereusedtoeharacterizetheireatalytiePerformanee.ResultsindicatedthattheeomPositePa
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