Chapter 4 Selective MRMs

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1、PesticideAnalyticalManualVol.IChapter1RegulatoryOperationsChapter2GeneralAnalyticalOperationsandInformationChapter3Chapter4MulticlassSelectiveMRMsMRMsChapter5GLCChapter6HPLCTableofContentspagedate401:MethodforN-MethylcarbamatesBasicReferences401-11/94Genera

2、lPrinciples401-11/94Applicability401-11/94ReferenceStandards401-11/94Stepsofthemethod401-11/94Validation401-21/94E1Extractionwithmethanol401-31/94E2Extractionwithmethanol,reducedsamplesize401-41/94C1Liquid-LiquidPartitioningandCharcoal/Celite401-51/94Column

3、CleanupDL1HPLC,Post-ColumnDerivatization,401-91/94FluorescenceDetectionTransmittalNo.96-E1(9/96)400–1FormFDA2905a(6/92)SECTION400PesticideAnalyticalManualVol.IpagedateDL2HPLC,FluorescenceDetection401-131/94Confirmation401-131/94402:MethodforAcidsandPhenolsB

4、asicReference402-11/94GeneralPrinciples402-11/94Applicability402-11/94ReferenceStandards402-11/94Stepsofthemethod402-11/94Validation402-21/94E1Extractionwithsolventsfromacidified,402-31/94denaturedproductsE2Extractionwithacidifiedmethylenechloride402-71/94E

5、3Extractionwithacidifiedmethanol402-91/94E4Extractionwithacidifiedwater/methanol402-101/94E5Extractionwithacidifiedmethanol402-111/94E6Dissolutioninmethylenechloride/hexane402-131/94E7Extractionwithacidifiedmethylenechloride402-151/94C1GPCCleanup,methylatio

6、n,andFlorisil402-171/94columncleanupC1aGPCCleanup402-171/94C1bMethylation402-211/94C1cFlorisilcolumncleanup402-221/94Determination402-251/94Confirmation402-251/94403:MethodforPhenylureaHerbicidesBasicReference403-11/94GeneralPrinciples403-11/94Applicability

7、403-11/94ReferenceStandards403-11/94Stepsofthemethod403-11/94Validation403-21/94E1ExtractionwithMethanol403-31/94C1Liquid-LiquidPartitioningandFlorisil403-51/94ColumnCleanupDL3HPLC,Post-ColumnPhotolysisand403-71/94Derivatization,FluorescenceDetectionDL4HPLC

8、,Differentmobilephase403-101/94Confirmation403-111/94404:MethodforBenzimidazolesBasicReference404-11/94GeneralPrinciples404-11/94400–2TransmittalNo.96-E1(9/96)FormFDA2905a(6/92)PesticideAnalyticalManua