无溶剂微波萃取没药精油及其在卷烟加香中的应用

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1、࿵Ҥ॓࠯/TobaccoScience&Technology࿵Ҥ߄࿐/TobaccoChemistry2014୍4௹čሹ321௹Ď໭ಷ࠴ັѯᑙ౼ીူࣚႲࠣఃᄝज࿵ࡆཐᇏႋႨ஌໓ਊđ಩ᆽ఼đਾѯđชޡབđჅଔފКᇏ࿵۽ြႵཋᄳ಩܄ඳ࠯ඌᇏྏđെࡅሌົૼଲնࢧ1050051ᅋေğҐႨ໭ಷ࠴ັѯᑙ౼مՖીူᇏิ౼ࣚႲđҩקਔః໾৘ྟᇉđ࡫קਔᇶေۿି๶đGC/MSمٳ༅ਔીူࣚႲᇶေ߄࿐Ӯٳđѩࣉྛਔज࿵ࡆཐ൫ဒbࢲݔіૼğæቋࡄᑙ౼่ࡱູીူٸෞ৬40ଢđ࣏೎ൈࡗ3hđັѯۿੱ800Wđᑙ౼ൈࡗ21minĠՎ่ࡱ༯ࣚႲੱູ3.95%bç܋࡫ק

2、ԛ62ᇕ߄ކ໾đᇶေЇওၳ໩ူ۴༖aᐹඌ༖a໩ူ۴༖aα-ϣଡ༖ބβ-ᢡཐ༖bèીူࣚႲିڿ೿ބྩ൥ज࿵࿵గđႵིࢆᄖగđڿ೿་໅ބჅ໅đࡨഒՏࠗbܱ࡯Սğ໭ಷ࠴ັѯᑙ౼ĠીူࣚႲĠज࿵ࡆཐᇏ๭щᅣ໓Bğ઒്ѓང໓3.264STğোٳğ1002-0861č2014Ď04-0060-05MyrrhEssentialOilPreparedbySolvent-freeMicrowaveExtractionanditsApplicationinTobaccoFlavoringPANWenliang,RENZhiqiang,LIUBo,TANHon

3、gxiang,andYUHanmouTechnologyCenter,ChinaTobaccoHebeiIndustrialCo.,Ltd.,Shijiazhuang050051,ChinaAbstract:TheMyrrhessentialoilwaspreparedwithsolvent-freemicrowaveextractionmethod.Itsphysicalpropertiesweremeasured,themainfunctionalgroupswereidentifiedandthemajorcomponentsint

4、heessentialoilwereanalyzedbyGC/MS.Theapplicationoftheessentialoilintobaccoflavoringwasevaluated.Theresultsshowedthat:1)Theoptimalextractingconditionswere:grindingto40mesh,soakingfor3hours,microwavepower800Wandextractingtime21minutes,underwhichtheyieldoftheextractwas3.95%.

5、2)Sixty-twocompoundswereidentifiedintheessentialoil,includingisolindestrene,curzerene,lindestrene,α-cedreneandβ-elemene,etc.3)Myrrhessentialoilcouldmodifyandimprovecigarettesmoke,reduceoffensiveodoreffectively,enhancesmokingtasteandaftertaste,andreduceirritation.Keywords:

6、Solvent-freemicrowaveextraction;Myrrhessentialoil;Tobaccoflavoringŀ4-5łીူູᣃᢡ॓ᆱ໾ھ֌đم਼ᆕగᆕඣູေᇶمٚ౼ิႲࣚူીႨӈĎlgnEmyrrharohpimmoCčඎנࠇିބ਽җ࠴ಷaӉࡗൈaۚ໑ႵऎمԢbᆫඎᄲۄĎlgnEmolmolarohpimmoCčඎנݗնಌbၘŀ6-7łႨቔཐਘຓđ္ႨႿ߄ሎ௖ބൊ௖bૅݓFDAᆣૼીႵӑਢࢸCO2ੀุᑙ౼مิ౼ીူࣚႲБđ෮ࣚŀ1łူႨቔٙཐเࡆ࠴ൊႨ൞νಆđFEMAູ2766ĠႲᇶေӮٳູα-ᑱ༖aβ-ѯக༖aβ

7、-ᢡཐ༖aّൔെGB2760i2011္ૼಒࡼીူႲਙູॖνಆ൐Ⴈൊᇰ༖aα-െᇰ༖aβ-ਟ༖aᢡཐԿaβ-ᢇွԿa؄඾ᅢ௖เࡆ࠴đщ൞N178ĠીူႲ္Фਙೆૅݓࠣႇݓॖଷބ༆ϣ༖b໭ಷ࠴ັѯᑙ౼مčSolvent-freeŀ2łνಆ൐Ⴈ࿵Ҥเࡆ࠴ྸॖ଀ֆᇏbીူᇏᇶေݣmicrowaveextraction,SFMEĎ൞၂ᇕྍ྘ᆱ໾ࣚႲิႵඎࢋč57%~65%Ďaඎᆫč25%~35%Ďaߨۄࠇ༷ྍಣࡆഝڕѯັႨ০෱đمٚ౼~%5.2čႲᄲ֌࣏ࣜ೎ŀ3ł9%Ďބ७໅෍ӮٳbીူᇶေࠃྟӮٳູࣚႲđԩ৘ᆱ໾ቆᆮđ๙ݖॹ෎చ߄ඣٳࡼቆᆮଽࣚ

8、Ⴒջԛđᄜࣜ৏ୠaٳ৖ުᆱ໾ࣚႲĠھٚمࡆቔᆀࡥࢺğ஌໓ਊč1974iĎđЧ॓đ۽ӱഽđᇶေՖ൙ཐࣚཐਘ࿹ಣ෎ٳӮ໅ཐđ؋ࡗൈಣ൳Ⴒࣚđॹ෥ാਈഒđ౏҂࣮ष۽ቔbE-mailğpwl3003@