蔓性千斤拔提取工艺与质量控制初步研究

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1、学校代码：10600学号：091087学位类型：科学学位广西中医药大学硕士学位论文蔓性千斤拔提取工艺与质量控制初步研究研究生：陈鹏导师：秦海洸教授院系（部所）：药学院专业：中药学研究方向：中药药性理论研究完成日期：2012年6月26日目录中文摘要···································································1Abstract·············································································3引言

2、·············································································6正文·············································································9第一部分蔓性千斤拔提取工艺研究·······································91星点设计-效应面法优化千斤拔提取工艺·································91.1试验材料与试验样品·

3、·······················································91.1.1材料···········································································91.1.2试剂···········································································91.1.3仪器··················································

4、·························91.1.4分析软件···································································101.2供试品溶液的制备·························································101.3对照品溶液的制备·························································101.4HPLC色谱条件························

5、·····································101.5标准曲线的绘制····························································111.6方法学考察··································································121.6.1精密度试验································································121.6.2稳定性试验······

6、··························································121.6.3重复性试验································································131.6.4加样回收率试验··························································131.7醇浸膏收率的测定·························································141

7、.8星点试验设计因素及数据处理··········································141.8.1星点设计···································································141.8.2模型拟合···································································151.8.4验证和放大试验····················································

8、······192正交设计试验优选千斤拔提取工艺·······················