头孢曲松钠小试报告(终)

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1、秘密华北制药河北华民药业有限责任公司《粒子过程晶体产品分子组装与形态优化技术科技成果转化项目基础研究》小试报告（头孢曲松钠）天津大学国家工业结晶研究推广中心二零一一年一月目录第一章前言..............................................11.1头孢曲松钠简介................................................11.2本报告内容....................................................2第二章头孢

2、曲松钠晶体结构表征与晶习预测........................32.1实验研究......................................................32.1.1晶体制备..................................................32.1.2晶体的分析表征............................................32.2结果与讨论......................................

3、..............52.2.1热分析....................................................52.2.2红外光谱分析..............................................62.2.3X-射线粉末衍射数据及其指标化..............................72.2.4头孢曲松钠晶体结构的确定.................................102.2.5头孢曲松钠晶习预测.............

4、..........................112.2.6结晶过程对头孢曲松钠晶习的影响...........................142.3小结.........................................................16第三章头孢曲松钠结晶热力学研究.............................183.1实验研究.....................................................183.1.1头孢曲松钠溶解度的测

5、定...................................183.1.2头孢曲松钠介稳区的测定...................................203.2结果与讨论...................................................203.2.1头孢曲松钠的溶解度.......................................203.2.2溶剂的选择...............................................

6、213.2.3头孢曲松钠溶解度数学模型的建立...........................233.2.4头孢曲松钠的介稳区.......................................263.5小结.........................................................27第四章头孢曲松钠成核、生长和聚结动力学研究...................294.1头孢曲松钠晶体生长机理辨识...................................2

7、94.1.1头孢曲松钠诱导期的测定...................................294.1.2结果与讨论...............................................304.2头孢曲松钠成核、生长、聚结动力学研究.........................314.2.1实验装置.................................................314.2.2实验步骤..................................

8、...............314.2.3数据预处理...............................................334.2.4实验结果与讨论...........................................334.3小结..............